View EntryDate of entry : 09/08/2016

Superspace description of trimethyltin hydroxide at T = 100 K
Dey, Somnath; Schoenleber, Andreas; Mondal, Swastik; van Smaalen, Sander Zeitschrift fur Kristallographie-Crystalline Materials 231(7) 427 - 434 (2016)

[ B-IncStrDB ID: 11792E3kVU6 ]
 
Submitted by : Luis Elcoro [UPV/EHU]CIF File

I

Commensurate Supercell Matrix

100
010
002

Chemical Properties

Structural Formula Sum: C3 H10 O1 Sn1   [Help]
Weight: 180.8 Daltons  [Help]

Crystallographic Properties

a: 6.65189(17) Å  [Help]
b: 10.6664(2) Å  [Help]
c: 4.14518(7) Å  [Help]
α: 90 °  [Help]
β: 90 °  [Help]
γ: 90 °  [Help]
Volume: 294.106(14) Å3  [Help]
Crystal System: orthorhombic   [Help]
Space Group Name: P21212(00γ)00s   [Help]
Number of Formula Units: 2   [Help]

  •  Additional Crystal Information   

Experimental Data

Absorption_coeff_μ: 2.192 &mm;  [Help]
Description of the crystal: needle   [Help]
Absorption-correction type: multi-scan   [Help]
Minimum transmission factor: 0.3016   [Help]
Maximum transmission factor: 0.4317   [Help]
Intensity Measure Temperature: 100(3) K  [Help]
Radiation Type: synchrotron   [Help]
Radiation Wavelength: 0.55999 Å  [Help]
Intensities measure method: φω   [Help]
Total measured intensities #: 9774   [Help]

  •  Additional Experimental Information   

Refinement Properties

Total # of reflections: 3273   [Help]
# of observed reflections: 3174   [Help]
Residual factor for the observed reflns.: 0.0215   [Help]

  •  Additional Refinement Information   

Diffraction Data

Intensity Measure Temperature: 100(3) K  [Help]
Nature of the radiation: X-ray   [Help]
Radiation Wavelength: 0.55999 Å  [Help]
_diffrn_measurement_device_type: MARCCD   [Help]

  •  Additional Diffraction Data Information   


  •  Reference Structure Information   

  •  Modulation Parameters (Tables)   

  •  Modulation Parameters (Atom Sites Summary)